Unit 2 & Unit 4 Chemistry

Redox Titrations

Notes:

Redox Titrations – 1

Redox Titrations – 2

Tests:

Redox Titrations – Topic Test 1

Redox Titrations – Topic Test 2

Pracs:

Determination of the Alcohol Content of Wine

Determination of the Iron (II) Content in Lawn Fertiliser by Redox Titration

Determination of Vitamin C Content in Tablets

The Concentration of Vitamin C in Various Substances Through Redox Titration

HPLC

Notes:

High Performance Liquid Chromatography

HPLC

Order of Elution of Sample Components

Worksheets:

Dynamic Science – Chromatography

Tests:

HPLC Concept Test

HPLC – Test 2

Pracs:

Determination of Caffeine in Soda

Determination of the Caffeine Content in Soft Drinks

Determination of the Caffeine Content in Commercial Tea Samples

Quantitative Analysis of Caffeine

Mixed Instrumental Techniques

Note: You may need the molecular weight of a compound in order to solve some questions.

Simply read the m/z value for the decently sized peak on the right hand side of the spectrum. In the below example, the answer is 32. Ignore tiny peaks like the one at m/z 33. Sometimes, you will get the answer wrong – but you will only be 1-2 amu from the true value. That should be enough information for you to solve these questions.

Notes:

Introduction to Structure Determination

Combination of Different Analytical Techniques to Determine Structure

Structure Determination

Worksheets:

Chemical Detectives – Spectra – Easy – Test 1

Chemical Detectives – Spectra – Easy – Test 2

Chemical Detectives – Spectra – Easy – Test 3

Chemical Detectives – Spectra – Medium – Test 1

Chemical Detectives – Spectra – Medium – Test 2

Chemical Detectives – Spectra – Hard – Test 1

Chemical Detectives – Spectra – Hard – Test 2

Topic 20 Exercise A – Combined Spectral Analysis